4-Phenylpiperazine-1-carboxylic acid (4,4-diethoxybutyl)amide → 4-Phenylpiperazine-1-carboxylic acid (4-oxobutyl)amide

HRID 1942373ノート

反応式

HRID 1942373 の反応式
C([O:3][CH:4](OCC)[CH2:5][CH2:6][CH2:7][NH:8][C:9]([N:11]1[CH2:16][CH2:15][N:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:13][CH2:12]1)=[O:10])C.O=CCCCNC(C1CCCCC1)=O>>[O:3]=[CH:4][CH2:5][CH2:6][CH2:7][NH:8][C:9]([N:11]1[CH2:12][CH2:13][N:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:15][CH2:16]1)=[O:10]

参加物

3

反応物 2

HCID 669375364-Phenylpiperazine-1-carboxylic acid (4,4-diethoxybutyl)amideHCID 85725969Cyclohexanecarboxylic acid (4-oxo-butyl)-amide

生成物 1

HCID 866513094-Phenylpiperazine-1-carboxylic acid (4-oxobutyl)amide

実験手順

4-Phenylpiperazine-1-carboxylic acid (4-oxobutyl)amide (61C) is prepared from 61B as described for 20B. The product is obtained in almost quantitative yield.

後処理

  1. customThe product is obtained in almost quantitative yield

出典と根拠

ORDレコード
ord-f3b89ee816344ddbbf4e68c4b58ff5cf
出典データセット
uspto-grants-2013_03
特許番号
US08389555B2

反応ノート

読み込み中…