Benzamide, N-(4-hydroxybutyl)- → 4-Phenyl-3,6-dihydro-2H-pyridine-1-carboxylic acid (4-hydroxybutyl)amide

HRID 1942376ノート

反応式

HRID 1942376 の反応式
[C:1]1([C:7]2[CH2:8][CH2:9][N:10]([C:13](Cl)=[O:14])[CH2:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH:16][CH2:17][CH2:18][CH2:19][CH2:20][NH:21]C(=O)C1C=CC=CC=1>>[OH:16][CH2:17][CH2:18][CH2:19][CH2:20][NH:21][C:13]([N:10]1[CH2:11][CH:12]=[C:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH2:8][CH2:9]1)=[O:14]

参加物

3

反応物 2

HCID 11217773Benzamide, N-(4-hydroxybutyl)-HCID 858108644-Phenyl-3,6-dihydro-2H-pyridine-1-carbonyl chloride

生成物 1

HCID 669374264-Phenyl-3,6-dihydro-2H-pyridine-1-carboxylic acid (4-hydroxybutyl)amide

実験手順

4-Phenyl-3,6-dihydro-2H-pyridine-1-carboxylic acid (4-hydroxybutyl)amide (62B) is prepared from 62A as described for 1D. The product is obtained in almost quantitative yield.

後処理

  1. customThe product is obtained in almost quantitative yield

出典と根拠

ORDレコード
ord-3d2647c7d9844d499a257e34f3032463
出典データセット
uspto-grants-2013_03
特許番号
US08389555B2

反応ノート

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