Trifluoromethanesulfonic acid, lithium salt → HCID 86595083、化合物

HRID 1954646ノート

反応式

HRID 1954646 の反応式
[CH:1]([C:9]1=[CH:10][C:11]([O:13][C:14]1=[O:15])=[O:12])=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.FC(F)(F)S([O-])(=O)=[O:19].[Li+]>CO>[CH:1](/[C:9](/[C:14]([OH:13])=[O:15])=[CH:10]/[C:11]([OH:19])=[O:12])=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

参加物

4

反応物 2

HCID 3664839Trifluoromethanesulfonic acid, lithium saltHCID 54215275Styrenemaleic anhydride

生成物 1

HCID 86595083HCID 86595083、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

反応条件

温度
100 °C

実験手順

0.5 g of the styrene-maleic anhydride polymer (molecular weight: 1600) was mixed with 1.5 g of polyethyleneoxyglycol (molecular weight: 600) and 0.5 g of lithium trifluoromethane sulfonate salt. The mixture was dropped on an ion-conducting glass electrode and heated in an oven at 100° C. under nitrogen stream. After 30 hours, the mixture was cooled to room temperature and immersed in methanol and dried. A thin membrane of styrene-maleic acid polyethyleneoxy ester copolymer of an excellent adhesive strength and mechanical strength was prepared. The ion conductivity of the polymer thin membrane prepared as above was 7×10-7S/cm at room temperature.

後処理

  1. additionThe mixture was dropped on an ion-conducting glass electrode
  2. temperaturethe mixture was cooled to room temperature
  3. customdried
  4. customThe ion conductivity of the polymer thin membrane prepared as
  5. customat room temperature

出典と根拠

ORDレコード
ord-c719652e0c454b9bb4a6b002d1425de1
出典データセット
uspto-grants-2000_09
特許番号
US06123875

反応ノート

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