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Tin tetrachloride → Tin hydroxide (Sn(OH)4)

HRID 1955472
ノート
印刷プレビュー

反応式

HRID 1955472 の反応式
[OH2:1].N.[Sn:3](Cl)(Cl)(Cl)Cl.[Sb:8](Cl)(Cl)Cl>O>[OH-:1].[Sn+4:3].[OH-:1].[OH-:1].[OH-:1].[OH-:1].[Sb+3:8].[OH-:1].[OH-:1]
参加物実験手順後処理出典と根拠反応ノート

参加物

6

反応物 3

HCID 24287Tin tetrachlorideHCID 24814Antimony trichlorideHCID 12896473Azane;hydrate

生成物 2

HCID 160964Tin hydroxide (Sn(OH)4)HCID 19362114Antimony hydroxide

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Tan et al. disclosed a process for the preparation of mixture powder containing tin and molybdenum oxides (Sn-Mo-O) (see J. of Catalysis, 17, 132-142(1970)). In their process, ammonia water was added into a water solution of tin tetrachloride to obtain tin hydroxide precipitate, which was then dispersed in the water solution of molybdenum ammonia. The binary oxide powder was finally obtained by drying the solution. Sala et al. disclosed a process for the preparation of Sn-Sb-O powder (see J. of Catalysis, 34, 68-78 (1974)). In this process, ammonia water was added the water solution of tin chloride and antimony chloride to obtain mixture precipitate of tin hydroxide and antimony hydroxide, which was then dried.

後処理

  1. customby drying the solution
  2. customfor the preparation of Sn-Sb-O powder (see J. of Catalysis, 34, 68-78 (1974))

出典と根拠

ORDレコード
ord-f6336af3ac8f47cbb1c7607cfb2041e5
出典データセット
uspto-grants-1998_07
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US05776425

反応ノート

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