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N-[1-(4'-Benzyloxybiphenyl-4-yl)-1-methylethyl]-3-(imidazol-1-yl)propylamine → 4'-{1-[3-(Imidazol-1-yl)propylamino]-1-methylethyl}biphenyl-4-ol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-[1-(4'-Benzyloxybiphenyl-4-yl)-1-methylethyl]-3-(imidazol-1-yl)propylamine | HCID 18349622 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 生成物 | 4'-{1-[3-(Imidazol-1-yl)propylamino]-1-methylethyl}biphenyl-4-ol | HCID 18349596 | — |
反応手順
N-[1-(4'-Benzyloxybiphenyl-4-yl)-1-methylethyl]-3-(imidazol-1-yl)propylamine was hydrogenated, using palladium on charcoal as catalyst, in IMS at atmospheric pressure to give 4'-{1-[3-(imidazol-1-yl)propylamino]-1-methylethyl}biphenyl-4-ol, m.p. 178°-180° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05780642 |
| 出典データセット | uspto-grants-1998_07 |
| ORD ID | ord-3181fb7a649645d18b2b436a0386a4ac |
| 出典メモ | uspto-grants-1998_07 |