1-Hydroxycyclohexyl phenyl ketone → Ethyl 4-(dimethylamino)benzoate

HRID 1968295

反応式

HRID 1968295 の反応式
[CH2:1]1[CH2:6][CH2:5][C:4](O)([C:7]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[O:8])[CH2:3][CH2:2]1.C[C:17](N1CCOCC1)([C:19](C1C=CC([S:27]C)=CC=1)=[O:20])C.[CH3:35][CH2:36][C:37](N(C)C)([C:45]([C:47]1[CH:52]=[CH:51][C:50]([N:53]2[CH2:58]COC[CH2:54]2)=[CH:49][CH:48]=1)=[O:46])CC1C=CC=CC=1.C1C=CC(C(C(OCCOCCOC(C(C2C=CC=CC=2)=O)=O)=O)=O)=CC=1>>[CH3:35][CH:36]([C:6]1[CH:1]=[CH:2][C:3]2[S:27][C:14]3[C:9]([C:7](=[O:8])[C:4]=2[CH:5]=1)=[CH:10][CH:11]=[CH:12][CH:13]=3)[CH3:37].[CH3:17][CH2:19][O:20][C:45]([C:47]1[CH:48]=[CH:49][C:50]([N:53]([CH3:54])[CH3:58])=[CH:51][CH:52]=1)=[O:46]

参加物

6

反応物 4

HCID 703551-Hydroxycyclohexyl phenyl ketoneHCID 861712-Benzyl-2-(dimethylamino)-1-(4-(morpholin-4-yl)phenyl)butan-1-oneHCID 923872-Methyl-1-(4-(methylthio)phenyl)-2-morpholino-1-propanoneHCID 60004985Benzeneacetic acid, alpha-oxo-, 1,1'-(oxydi-2,1-ethanediyl) ester

生成物 2

HCID 25127Ethyl 4-(dimethylamino)benzoateHCID 796332-Isopropylthioxanthone

実験手順

Specific examples include such as Irgacure 184, Irgacure 907, Irgacure 369, Irgacure 379, Irgacure 819, Irgacure 127, Irgacure 500, Irgacure 754, Irgacure 250, Irgacure 1800, Irgacure 1870, Irgacure OXE01, DAROCUR TPO and DAROCUR 1173, produced by Ciba Specialty Chemicals K. K.; Speedcure MBB, Speedcure PBZ, Speedcure ITX, Speedcure CTX, Speedcure EDB, Esacure ONE, Esacure KIP150, and Esacure KTO46, produced by Nihon SiberHegner K. K.; and KAYACURE DETX-S, KAYACURE CTX, KAYACURE BMS and KAYACURE DMBI, produced by Nippon Kayaku Co., Ltd. An amount of the photopolymerization initiator to be added is preferably 0.1 to 10 parts by weight with respect to 100 parts by weight of the ionizing radiation-curable resin.

後処理

  1. customproduced by Ciba Specialty Chemicals K

出典と根拠

ORDレコード
ord-b24ffc52afa3451a8935945cb157b228
出典データセット
uspto-grants-2013_04
特許番号
US08422133B2

関連ノート

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