関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | (2-Amino-2,3-dihydro-1H-inden-2-yl)methanol | HCID 22080542 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 2-(2-Hydroxymethylindan-2-yl)-isoindole-1,3-dione | HCID 68561206 | — |
反応手順
A mixture of (2-aminoindan-2-yl)methanol (0.407 g, 2.50 mmol) and phthalic anhydride (0.369 g, 2.50 mmol) is heated at 160° C. for 40 minutes. The reaction mixture is poured into water and extracted with chloroform. The organic phase is dried (Na2SO4) and evaporated to afford 2-(2-hydroxymethylindan-2-yl)-isoindole-1,3-dione, MH+294.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07745462B2 |
|---|
| 出典データセット | uspto-grants-2010_06 |
|---|
| ORD ID | ord-9c2a51c334da45ef9b380da3998da7ac |
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| 出典メモ | uspto-grants-2010_06 |
|---|
