N-(2-Chloroethyl)-N-ethylaniline → N,N-dimethyl-N-2-(N'-ethylanilino)ethyl-N-2-hydroxyethylammonium chloride
反応式
[CH3:1][N:2]([CH2:4][CH2:5][OH:6])[CH3:3].[CH2:7]([N:9]([CH2:16][CH2:17][Cl:18])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH3:8]>O>[Cl-:18].[CH3:1][N+:2]([CH3:3])([CH2:17][CH2:16][N:9]([CH2:7][CH3:8])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH2:4][CH2:5][OH:6]参加物
4
実験手順
A stirred mixture of 35.6 parts of dimethylaminoethanol in 60 parts of water was heated to 90° and 73.6 parts of N-ethyl-N-(2-chloroethyl)aniline was gradually added. The mixture was heated at 90°-95°. After two and one-half hours there was obtained N,N-dimethyl-N-2-(N'-ethylanilino)ethyl-N-2-hydroxyethylammonium chloride in the form of an aqueous solution.
後処理
- temperaturewas heated to 90°
- temperatureThe mixture was heated at 90°-95°
出典と根拠
- ORDレコード
- ord-200204880b1d4ea29c6d64112f0ec5c0
- 出典データセット
- uspto-grants-1976_12
- 特許番号
- US03996282
反応ノート
読み込み中…