関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Formaldehyde | HCID 712 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Thiophen-2-acetamide | HCID 78208 | — |
| 生成物 | N-(Hydroxymethyl)-2-(thiophen-2-yl)acetamide | HCID 21452354 | — |
反応手順
A mixture of 2-thienylacetamide, formaldehyde solution (37%, 1 equivalent) and a catalytic amount of potassium carbonate is warmed on a steam bath until a homogeneous solution is obtained. The solution is cooled to 0° C. overnight and the resulting solid collected by filtration.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US03997527 |
|---|
| 出典データセット | uspto-grants-1976_12 |
|---|
| ORD ID | ord-0406e70fb2c645fcab15b228c717d585 |
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| 出典メモ | uspto-grants-1976_12 |
|---|
