{2-[(Chloromethyl)sulfanyl]propan-2-yl}benzene → HCID 21489059、化合物

HRID 1974244ノート

反応式

HRID 1974244 の反応式
[CH3:1][C:2]([S:10][CH2:11]Cl)([CH3:9])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[P:13]([S-:19])(=[S:18])([O:16][CH3:17])[O:14][CH3:15].[Na+]>CC(C)=O>[P:13]([S:19][CH2:11][S:10][C:2]([CH3:9])([CH3:1])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1)(=[S:18])([O:16][CH3:17])[O:14][CH3:15]

参加物

4

反応物 2

HCID 21489039{2-[(Chloromethyl)sulfanyl]propan-2-yl}benzeneHCID 23683120Phosphorodithioic acid, O,O-dimethyl ester, sodium salt

生成物 1

HCID 21489059HCID 21489059、化合物

試薬・触媒・溶媒 1

HCID 180Acetone溶媒

実験手順

To 0.078 mole of chloromethyl α,α-dimethylbenzyl sulfide in 100 ml. of acetone is added 15.3 grams (0.078 mole) of sodium O,O-dimethyl phosphorodithioate followed by stirring overnight. The reaction mixture is maintained at a temperature of 25° C. to 30° C.

後処理

  1. temperatureThe reaction mixture is maintained at a temperature of 25° C. to 30° C.

出典と根拠

ORDレコード
ord-660ab75a5c3043d2bbefa5702c3d4a7c
出典データセット
uspto-grants-1976_12
特許番号
US04000269

反応ノート

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