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Chloroform → HCID 18766188、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chloroform | HCID 6212 | — |
| 反応物 | n-Heptyl isocyanate | HCID 138341 | — |
| 反応物 | 1-(Aminooxy)-3-(piperidin-1-yl)propan-2-ol | HCID 18766210 | — |
| 生成物 | HCID 18766188 | HCID 18766188 | — |
反応手順
To the solution of 1.23 g (7.1 mmol) of l-aminooxy-2-hydroxy-3-(1-piperidinyl)-propane dissolved in 20 ml of chloroform 1.0 g (7.1 mmol) of heptyl isocyanate was added and the reaction mixture was stirred for 20 hours. Solvent was evaporated in vacuum and the residue was purified by chromatography to give pure colorless oil. White crystalline product was obtained by triturating with petroleum ether.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07745465B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-5d41a87368eb46de9294345e9b841d10 |
| 出典メモ | uspto-grants-2010_06 |