化工社化工社 化学情報印刷レポート · 研究参考用
1-(Chloromethoxy)-2-methoxyethane → CD 2665
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(Chloromethoxy)-2-methoxyethane | HCID 77590 | — |
| 反応物 | Methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate | HCID 22000367 | — |
| 生成物 | CD 2665 | HCID 216241 | 55.7% |
反応手順
Following the procedure of Example 1(a), but reacting 980 mg (2.4 mmol) of methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 330 μl (28.6 mmol) of methoxyethoxymethyl chloride, 650 mg (55%) of the expected compound were obtained in the form of an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06225328B1 |
| 出典データセット | uspto-grants-2001_05 |
| ORD ID | ord-c9815e2a0dad460584c6bf88cb4ad2ff |
| 出典メモ | uspto-grants-2001_05 |