Methyl trifluoroacetate → HCID 10535860、化合物
反応式
[NH2:1][CH:2]1[CH2:6][CH2:5][NH:4][C:3]1=[O:7].[F:8][C:9]([F:15])([F:14])[C:10](OC)=[O:11]>CO>[F:8][C:9]([F:15])([F:14])[C:10]([NH:1][CH:2]1[CH2:6][CH2:5][NH:4][C:3]1=[O:7])=[O:11]参加物
4
実験手順
A suspension of Intermediate 2 (181 g), methyl trifluoroacetate (218 ml) and methanol (2.6 l) was stirred for 2 h. The solvent was then removed in vacuo to afford the title compound as a cream solid (355 g). Mass spec. MNH4+ (found) 214 MNH4+ (calculated) 214
後処理
- customThe solvent was then removed in vacuo
出典と根拠
- ORDレコード
- ord-562212bbe1ae4a95a094ec7d441fbaf2
- 出典データセット
- uspto-grants-2001_05
- 特許番号
- US06228853B1
反応ノート
読み込み中…