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2-Bromo-6-methylbenzoic acid → 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[(2-bromo-6-methylphenyl)carbonyl]-L-phenylalanine methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromo-6-methylbenzoic acid | HCID 2735589 | — |
| 反応物 | 4-(2,6-Dichlorobenzoylamino)-L-phenylalanine methyl ester | HCID 23383933 | — |
| 生成物 | 4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[(2-bromo-6-methylphenyl)carbonyl]-L-phenylalanine methyl ester | HCID 53758850 | 64% |
反応手順
4-[[(2,6-Dichlorophenyl)carbonyl]amino]-N-[(2-bromo-6-methylphenyl)carbonyl]-L-phenylalanine methyl ester was prepared in 64% yield from 4-[[(2,6-dichlorophenyl)carbonyl]amino]-L-phenylalanine methyl ester and 2-bromo-6-methylbenzoic acid using the general procedure described in example 3. HR MS: Obs. mass, 563.0138. Calcd. mass, 563.0140 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06229011B1 |
| 出典データセット | uspto-grants-2001_05 |
| ORD ID | ord-de1e3a1fcaa5424f9d6366fdd122164d |
| 出典メモ | uspto-grants-2001_05 |