3,5-Di-tert-butyl-4-hydroxybenzaldehyde → 2-(1,1-Dimethylethyl)-6-methyl-4-(1-piperazinylmethyl)phenol

HRID 1977129

反応式

HRID 1977129 の反応式
C[C:2]([C:5]1[CH:6]=[C:7]([CH2:16][N:17]2[CH2:22][CH2:21][NH:20][CH2:19][CH2:18]2)[CH:8]=[C:9]([C:12]([CH3:15])([CH3:14])[CH3:13])[C:10]=1[OH:11])(C)C.CC(C1C=C(C=C(C)C=1O)C=O)(C)C.CC(C1C=C(C=C(C(C)(C)C)C=1O)C=O)(C)C>>[CH3:15][C:12]([C:9]1[CH:8]=[C:7]([CH2:16][N:17]2[CH2:18][CH2:19][NH:20][CH2:21][CH2:22]2)[CH:6]=[C:5]([CH3:2])[C:10]=1[OH:11])([CH3:13])[CH3:14]

参加物

4

反応物 3

HCID 732193,5-Di-tert-butyl-4-hydroxybenzaldehydeHCID 124679863-tert-Butyl-4-hydroxy-5-methylbenzaldehydeHCID 128958282,6-Di-tert-butyl-4-[(piperazin-1-yl)methyl]phenol

生成物 1

HCID 219977902-(1,1-Dimethylethyl)-6-methyl-4-(1-piperazinylmethyl)phenol

実験手順

This was prepared using the general methodology described for the preparation of 1-(3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl)methylpiperazine except that 3-(1,1-dimethylethyl)-4-hydroxy-5-methylbenzaldehyde replaced the 3,5-bis(1,1-dimethylethyl)-4-hydroxybenzaldehyde.

後処理

  1. customThis was prepared

出典と根拠

ORDレコード
ord-3a6afa8eaeee4e318d2d422f9f6420e1
出典データセット
uspto-grants-2001_05
特許番号
US06232314B1

関連ノート

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