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2-Bromopyridine → 2-methoxy-N-(2-pyridyl)acetanilide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Bromopyridine | HCID 7973 | — |
| 反応物 | 2-methoxy-N-phenylacetamide | HCID 264222 | — |
| 生成物 | 2-methoxy-N-(2-pyridyl)acetanilide | HCID 21993568 | 58.6% |
反応手順
Using 2-methoxy-acetanilide (5.0 g) and 2-bromopyridine (9.5 g), a reaction was made in the same manner as in 1) of Production Example 14. The subsequent purification by silica gel column chromatography (developing solvent, ethyl acetate: hexane=1:1) produced 2-methoxy-N-(2-pyridyl)acetanilide (4.3 g, crude product) as a yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06235730B1 |
| 出典データセット | uspto-grants-2001_05 |
| ORD ID | ord-162c1cd072634f41b05a44072b02e280 |
| 出典メモ | uspto-grants-2001_05 |