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5,7-Dimethyladamantane-1,3-diol → 1,3-Dimethyl-5-hydroxy-7-acryloyloxyadamantane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5,7-Dimethyladamantane-1,3-diol | HCID 580605 | — |
| 反応物 | 1-Hydroxy-3-(acryloyloxymethyl)adamantane | HCID 21996783 | — |
| 生成物 | 1,3-Dimethyl-5-hydroxy-7-acryloyloxyadamantane | HCID 22228788 | 87% |
反応手順
The reaction was conducted in the same manner as the step of Example 36 (2) except that 1,3-dimethyl-5,7-dihydroxyadamantane was used instead of the 1,3-dicarboxy-5-adamantanol, and, as a result, a 1,3-dimethyl-5-hydroxy-7-acryloyloxyadamantane (yield: 87%, white solid) was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06235851B1 |
| 出典データセット | uspto-grants-2001_05 |
| ORD ID | ord-6c67c3a798b54d3a8126d39f48f5fced |
| 出典メモ | uspto-grants-2001_05 |