2,4-Dichlorobenzoic Acid → 4-Chloro-2-((4-methoxyphenyl)amino)benzoic acid

HRID 1980490

反応式

HRID 1980490 の反応式
Cl[C:2]1[CH:10]=[C:9]([Cl:11])[CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[CH3:12][O:13][C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[CH:16][CH:15]=1>>[Cl:11][C:9]1[CH:8]=[CH:7][C:3]([C:4]([OH:6])=[O:5])=[C:2]([NH:18][C:17]2[CH:19]=[CH:20][C:14]([O:13][CH3:12])=[CH:15][CH:16]=2)[CH:10]=1

参加物

3

反応物 2

HCID 57872,4-Dichlorobenzoic AcidHCID 7732P-Anisidine

生成物 1

HCID 666744-Chloro-2-((4-methoxyphenyl)amino)benzoic acid収率 60%

実験手順

4-Chloro-2-(4-methoxyphenylamino)benzoic acid [VII; R=4--Cl, R"=H, OR°=4--OCH3 ] was prepared from 2,4-dichlorobenzoic acid and 4-methoxyaniline according to the procedure of Example 1, part (a), and was obtained in about 60% yield as a green-grey solid.

後処理

  1. customwas obtained in about 60% yield as a green-grey solid

出典と根拠

ORDレコード
ord-efba26ae81c5471a966935a24e92d55a
出典データセット
uspto-grants-1985_04
特許番号
US04510139

関連ノート

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