3-Pyridinemethanamine → 3-Methoxy-4-(3-pyridyl)methylamino-1,2,5-thiadiazole 1-oxide
反応式
[NH2:1][CH2:2][C:3]1[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=1.[CH3:9][O:10][C:11]1[C:15](OC)=[N:14][S:13](=[O:18])[N:12]=1>CO>[CH3:9][O:10][C:11]1[C:15]([NH:1][CH2:2][C:3]2[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=2)=[N:14][S:13](=[O:18])[N:12]=1参加物
4
実験手順
A solution of 3-aminomethylpyridine (2.02 g; 18.7 mmoles) in 80 ml of methanol was added dropwise over 40 minutes to a partial suspension of 3,4-dimethoxy-1,2,5-thiadiazole 1-oxide (3.03 g; 18.7 mmoles) in 150 ml of methanol, to produce a methanol solution of the title compound.
出典と根拠
- ORDレコード
- ord-fbee0509122546a895eafdc1bc910103
- 出典データセット
- uspto-grants-1985_04
- 特許番号
- US04510309
反応ノート
読み込み中…