Methylhydrazine → (Aminomethylamino)((4-chlorophenyl)amino)methane-1-thione
反応式
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]=[C:9]=[S:10])=[CH:4][CH:3]=1.[CH3:11][NH:12][NH2:13]>C(O)C>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]([N:12]([CH3:11])[NH2:13])=[S:10])=[CH:4][CH:3]=1参加物
4
実験手順
A mixture of 4-chlorophenylisothiocyanate (17.0 g, 0.10 mole) and methylhydrazine (5.0 g, 0.11 mole) in 80 ml of ethanol was stirred at room temperature for two hours. The reaction mixture was filtered to collect colorless crystalline N-(4-chlorophenyl)-1-methylhydrazinecarbothioamide (18.4 g, mp 152°-154° C.).
後処理
- filtrationThe reaction mixture was filtered
- customto collect colorless crystalline N-(4-chlorophenyl)-1-methylhydrazinecarbothioamide (18.4 g, mp 152°-154° C.)
出典と根拠
- ORDレコード
- ord-6d4d2704efcb46fc958055c8e078625f
- 出典データセット
- uspto-grants-1985_04
- 特許番号
- US04514419
反応ノート
読み込み中…