化工社化工社 化学情報印刷レポート · 研究参考用
Toluene → Oleylamine styrene oxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Toluene | HCID 1140 | — |
| 反応物 | Styrene Oxide | HCID 7276 | — |
| 反応物 | Oleylamine | HCID 5356789 | — |
| 反応物 | Boron | HCID 5462311 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Oleylamine styrene oxide | HCID 86740542 | — |
反応手順
A sulfurized, boron-containing, heterocyclic compound is prepared by mixing 12 grams of oleylamine, 9.6 grams of styrene oxide and 200 ml of toluene for 30 minutes at room temperature (25° C.) in a single-necked one-liter round-bottomed flask. The flask is placed in a heating mantle and equipped with a water-cooled condenser. The mixture is heated under reflux for three hours producing an oleylamine/styrene oxide adduct.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04595514 |
| 出典データセット | uspto-grants-1986_06 |
| ORD ID | ord-80e74dfb277c499ea67e61ae01fcddfc |
| 出典メモ | uspto-grants-1986_06 |