関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethyl Bromide | HCID 6332 | — |
| 反応物 | 1,3-Dibromopropane | HCID 8001 | — |
| 反応物 | Triethyl phosphite | HCID 31215 | — |
| 生成物 | Diethyl (3-bromopropyl)phosphonate | HCID 283500 | — |
反応手順
A mixture of 605 g (3.0 mol) of 1,3-dibromopropane and 250 g (1.5 mol) of triethyl phosphite was heated at an oil bath temperature of 130° C., while stirring and passing in nitrogen, for approximately 5 hours until approximately 154 g (1.5 mol) of bromoethane distilled over into a strongly ice-cooled receiver. The reaction mixture was distilled first in a bulb tube and then fractionally.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05728686 |
|---|
| 出典データセット | uspto-grants-1998_03 |
|---|
| ORD ID | ord-0e2048f259f14c369c409d485f3d1e95 |
|---|
| 出典メモ | uspto-grants-1998_03 |
|---|
