2,4,5-Trichloropyrimidine → HCID 86625360、化合物

反応式

[CH3:1][O:2][C:3]([C:5]1[C:13]2[CH:12]=[C:11]([C:14]3[CH:19]=[CH:18][N:17]=[C:16]([Cl:20])[N:15]=3)[S:10][C:9]=2[CH:8]=[CH:7][CH:6]=1)=[O:4].COC(C1C2C=CSC=2C=CC=1)=O.[Cl:34]C1N=C(Cl)C(Cl)=CN=1>>[CH3:1][O:2][C:3]([C:5]1[C:13]2[CH:12]=[C:11]([C:14]3[C:19]([Cl:34])=[CH:18][N:17]=[C:16]([Cl:20])[N:15]=3)[S:10][C:9]=2[CH:8]=[CH:7][CH:6]=1)=[O:4]

参加物

反応物 3

HCID 2372592,4,5-Trichloropyrimidine

HCID 13448678Methyl 1-benzothiophene-4-carboxylate

HCID 86625361HCID 86625361、化合物

生成物 1

HCID 86625360HCID 86625360、化合物

実験手順

Using the method of 2-(2-chloropyrimidin-4-yl)-benzo[b]thiophene-4-carboxylic acid methyl ester, the title compound is synthesized from benzo[b]thiophene-4-carboxylic acid methyl ester and 2,4,5-trichloropyrimidine and isolated as a solid.