2-(2-Chlorophenyl)propan-2-amine → HCID 57722624、化合物

反応式

[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]([NH2:11])([CH3:10])[CH3:9].Cl[C:13]1[N:18]=[C:17]([S:19][C:20]#[N:21])[C:16]([N+:22]([O-:24])=[O:23])=[CH:15][N:14]=1>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]([NH:11][C:13]1[N:18]=[C:17]([S:19][C:20]#[N:21])[C:16]([N+:22]([O-:24])=[O:23])=[CH:15][N:14]=1)([CH3:9])[CH3:10]

参加物

反応物 2

HCID 105351472-(2-Chlorophenyl)propan-2-amine

HCID 210775882-Chloro-5-nitropyrimidin-4-yl thiocyanate

生成物 1

HCID 57722624HCID 57722624、化合物

実験手順

[1-(2-Chlorophenyl)-1-methyl-ethyl]-(5-nitro-4-thiocyanato-pyrimidin-2-yl)-amine was prepared by addition of the above amine to 2-chloro-5-nitro-4-thiocyanato-pyrimidine using the procedure described in Example 17. m/z calcd. C14H11N5O2S [M−H]−: 348.79. Found: 348.05.

出典と根拠

ORDレコード: ord-f19156e04830427fb8f2e105ab0f3026
出典データセット: uspto-grants-2009_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07550473B2

反応ノート

読み込み中…