4-Chlorobenzyl alcohol → 4-[(4-Chlorophenyl)methoxy]-3-nitropyridine
反応式
Cl[C:2]1[CH:7]=[CH:6][N:5]=[CH:4][C:3]=1[N+:8]([O-:10])=[O:9].[Cl:11][C:12]1[CH:19]=[CH:18][C:15]([CH2:16][OH:17])=[CH:14][CH:13]=1>>[Cl:11][C:12]1[CH:19]=[CH:18][C:15]([CH2:16][O:17][C:2]2[CH:7]=[CH:6][N:5]=[CH:4][C:3]=2[N+:8]([O-:10])=[O:9])=[CH:14][CH:13]=1参加物
3
実験手順
In accordance with the same procedures as in Preparation 2, except for using 4-chloro-3-nitropyridine prepared in Step 1 of Preparation 1 and 4-chlorobenzyl alcohol, the titled compound was obtained as a white solid. (Yield: 78.0%)
後処理
- customIn accordance with the same procedures as in Preparation 2
出典と根拠
- ORDレコード
- ord-0e2bd51a65b94b20b9d409262b107226
- 出典データセット
- uspto-grants-2010_01
- 特許番号
- US07642269B2
反応ノート
読み込み中…