Benzoyl chloride → N-[4-(5-cyano-1-methyl-1H-pyrrol-2-yl)phenyl]benzamide
反応式
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[N:12]([CH3:13])[C:11]([C:14]#[N:15])=[CH:10][CH:9]=2)=[CH:4][CH:3]=1.[C:16](Cl)(=[O:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:14]([C:11]1[N:12]([CH3:13])[C:8]([C:5]2[CH:6]=[CH:7][C:2]([NH:1][C:16](=[O:23])[C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[CH:3][CH:4]=2)=[CH:9][CH:10]=1)#[N:15]参加物
3
実験手順
The title compound was prepared according to the general procedure for acylation of 5-(4-aminophenyl)-1-methyl-1H-pyrrole-2-carbonitrile using benzoyl chloride (64 μL, 0.55 mmol) to provide N-[4-(5-cyano-1-methyl-1H-pyrrol-2-yl)phenyl]benzamide (0.035 g).
後処理
- customThe title compound was prepared
出典と根拠
- ORDレコード
- ord-1f4303ae3f9144169262b0ad84d08616
- 出典データセット
- uspto-grants-2010_01
- 特許番号
- US07652062B2
反応ノート
読み込み中…