Hydrochloric Acid → HCID 86606498、化合物
反応式
[CH3:1][O:2][CH2:3][C@@H:4]([NH:14]C(=O)OC(C)(C)C)[CH2:5][NH:6]C(=O)OC(C)(C)C.[ClH:22].CCOCC>CO>[ClH:22].[ClH:22].[CH3:1][O:2][CH2:3][C@@H:4]([NH2:14])[CH2:5][NH2:6]参加物
5
実験手順
To a solution of di-tert-butyl [(2S)-3-methoxypropane-1,2-diyl]biscarbamate (895 mg, 2.94 mmol) in MeOH (30 mL), was added 2N HCl in Et2O (15 mL, 29.4 mmol). The reaction was stirred at rt for 18 h and the solvents evaporated to yield the title compound as a white solid (478 mg, 92%). LCMS: (FA) ES+ 105.0 (M+1).
後処理
- customthe solvents evaporated
出典と根拠
- ORDレコード
- ord-b3e21e47e2624ec1b97526b8155a2b5e
- 出典データセット
- uspto-grants-2010_01
- 特許番号
- US07652041B2
反応ノート
読み込み中…