化工社化工社 化学情報印刷レポート · 研究参考用
Formic Acid → Pinacol monoformate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | Hydrogen Peroxide | HCID 784 | — |
| 反応物 | Pinacol | HCID 6425 | — |
| 反応物 | 2,3-Dimethyl-1-butene | HCID 11249 | — |
| 生成物 | Pinacol monoformate | HCID 123559 | — |
反応手順
A process for preparing 2,3-dimethyl-2,3-butandiol which comprises introducing into a reaction vessel containing formic acid at 50° to 70° C. while stirred, 2,3-dimethylbutene and hydrogen peroxide, said 2,3-dimethylbutene and hydrogen peroxide being introduced into said formic acid simultaneously but separately and thereafter hydrolyzing pinacol monoformate so formed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04404410 |
| 出典データセット | uspto-grants-1983_09 |
| ORD ID | ord-69c77eb257cb41cbabc2a4329efc457a |
| 出典メモ | uspto-grants-1983_09 |