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Triethyl phosphite → 5-(Diethylphosphono)pentyl acetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethyl phosphite | HCID 31215 | — |
| 反応物 | 5-Bromopentyl acetate | HCID 85140 | — |
| 生成物 | 5-(Diethylphosphono)pentyl acetate | HCID 19689222 | — |
反応手順
100.34 g (0.48 mol) of 5-bromopentyl acetate were heated at 150° C. for 8 hours with 79.8 g (0.048 mol) of triethyl phosphite while stirring and passing in nitrogen. The mixture was then fractionally distilled under reduced pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05728686 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-37e8c73db5a4451484b91a4dd3cc9bb3 |
| 出典メモ | uspto-grants-1998_03 |