化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Carbonate → Diethyl 5-hydroxypentylphosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | 5-(Diethylphosphono)pentyl acetate | HCID 19689222 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Diethyl 5-hydroxypentylphosphonate | HCID 10680635 | — |
反応手順
92 g (0.345 mol) of 5-(diethylphosphono)pentyl acetate were heated at 50° C. for 10 hours with stirring with 74 g (0.7 mol) of finely powdered sodium carbonate in 500 ml of methanol. The solution was filtered, concentrated and distilled in a bulb tube.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05728686 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-c88ff47b784b42e596807b91fc6e4cda |
| 出典メモ | uspto-grants-1998_03 |