化工社化工社 化学情報印刷レポート · 研究参考用
1-Bromopropane → Diethyl [4-(3-ethyl-7-propylxanthin-1-yl)butyl]phosphonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Bromopropane | HCID 7840 | — |
| 反応物 | Diethyl [4-(3-ethyl-xanthin-1-yl)butyl]phosphonate | HCID 22446291 | — |
| 生成物 | Diethyl [4-(3-ethyl-7-propylxanthin-1-yl)butyl]phosphonate | HCID 22446286 | — |
反応手順
The title substance was prepared from 8.2 mmol of diethyl [4-(3-ethyl-xanthin-1-yl)butyl]phosphonate and 9.8 mmol of bromopropane analogously to Example 30 and chromatographed on silica gel (eluent: dichloromethane/methanol 20:1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05728686 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-6f7760bc41454f178cfc2b916e1815a1 |
| 出典メモ | uspto-grants-1998_03 |