3-(3-Chlorophenyl)-2-propynal → 3-(3-Chlorophenyl)prop-2-ynal oxime

HRID 2040862ノート

反応式

HRID 2040862 の反応式
[C:1]1([C:7]#[C:8][CH:9]=[N:10][OH:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:12]C1C=C(C#CC=O)C=CC=1>>[Cl:12][C:3]1[CH:2]=[C:1]([C:7]#[C:8][CH:9]=[N:10][OH:11])[CH:6]=[CH:5][CH:4]=1

参加物

3

反応物 2

HCID 468725403-(3-Chlorophenyl)-2-propynalHCID 765430553-Phenylprop-2-ynal oxime

生成物 1

HCID 765430563-(3-Chlorophenyl)prop-2-ynal oxime収率 96.4%

実験手順

The title compound was prepared following the method here described for Compound 1a, using Compound 31d instead of phenylpropiolaldehyde. The pale brown residue was used in the next step without further purification. Yield: 96.4%.

後処理

  1. customThe pale brown residue was used in the next step without further purification

出典と根拠

ORDレコード
ord-a3b51d3f27f14f879e822be58fb81423
出典データセット
uspto-grants-2013_11
特許番号
US08580962B2

反応ノート

読み込み中…