3-(m-Tolyl)propiolaldehyde → N-hydroxy-3-(3-methylphenyl)prop-2-yn-1-imine

HRID 2040888ノート

反応式

HRID 2040888 の反応式
Cl[C:2]1[CH:3]=[C:4]([C:8]#[C:9][CH:10]=[N:11][OH:12])[CH:5]=[CH:6][CH:7]=1.[CH3:13]C1C=C(C#CC=O)C=CC=1>>[OH:12][N:11]=[CH:10][C:9]#[C:8][C:4]1[CH:5]=[CH:6][CH:7]=[C:2]([CH3:13])[CH:3]=1

参加物

3

反応物 2

HCID 107731013-(m-Tolyl)propiolaldehydeHCID 765430563-(3-Chlorophenyl)prop-2-ynal oxime

生成物 1

HCID 86662876N-hydroxy-3-(3-methylphenyl)prop-2-yn-1-imine

実験手順

The title compound was synthesized following the procedure reported for Compound 31e but starting from Compound 91b instead of Compound 31d. The crude title compound (brownish oil) was used in the next step without further purification.

後処理

  1. customThe crude title compound (brownish oil) was used in the next step without further purification

出典と根拠

ORDレコード
ord-740331082d32413fb3a8b9f2ace8b25a
出典データセット
uspto-grants-2013_11
特許番号
US08580962B2

反応ノート

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