化工社化工社 化学情報印刷レポート · 研究参考用
Aniline → N-phenyl-2-Dibenzofuranamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Ethyl Acetate | HCID 8857 | — |
| 反応物 | 2-Iododibenzofuran | HCID 223327 | — |
| 溶媒 | Hexane | HCID 8058 | — |
| 生成物 | N-phenyl-2-Dibenzofuranamine | HCID 67204676 | — |
反応手順
The Rf values of the objective substance, 2-iododibenzofuran, and aniline were respectively 0.28, 0.59, and 0.07, which were found by silica gel thin layer chromatography (TLC) (with a developing solvent of ethyl acetate and hexane in a ratio of 1:10).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08580980B2 |
| 出典データセット | uspto-grants-2013_11 |
| ORD ID | ord-4184c7be028a4bc1bb941d5e1b8ce571 |
| 出典メモ | uspto-grants-2013_11 |