Pentaerythritol Tetranitrate → 2,2-Bis[(nitrooxy)methyl]propane-1,3-diyl dinitrate--2-methyl-1,3,5-trinitrobenzene (1/1)

HRID 2041796

反応式

HRID 2041796 の反応式
[CH3:1][C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][C:5]([N+:11]([O-:13])=[O:12])=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15].[CH2:17]([O:34][N+:35]([O-:37])=[O:36])[C:18]([CH2:29][O:30][N+:31]([O-:33])=[O:32])([CH2:24][O:25][N+:26]([O-:28])=[O:27])[CH2:19][O:20][N+:21]([O-:23])=[O:22]>>[CH2:29]([O:30][N+:31]([O-:33])=[O:32])[C:18]([CH2:19][O:20][N+:21]([O-:23])=[O:22])([CH2:17][O:34][N+:35]([O-:37])=[O:36])[CH2:24][O:25][N+:26]([O-:28])=[O:27].[CH3:1][C:2]1[C:7]([N+:8]([O-:10])=[O:9])=[CH:6][C:5]([N+:11]([O-:13])=[O:12])=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15]

参加物

3

反応物 2

HCID 6518Pentaerythritol TetranitrateHCID 83762,4,6-Trinitrotoluene

生成物 1

HCID 568417792,2-Bis[(nitrooxy)methyl]propane-1,3-diyl dinitrate--2-methyl-1,3,5-trinitrobenzene (1/1)

反応条件

温度
95 °C

実験手順

Briefly, a quantity of TNT were added and heated at 95° C. until melting in a reactor provided with a heating jacket and with mechanical stifling. Then, a quantity of PETN were added with a quantity of a gum [e.g., xanthan gum or guar gum] and a quantity of a wax. The components were stirred until achieving a homogeneous mixture which was poured on a cylindrical mold and left to cool, in order to obtain a composition of PETN/TNT/gum/wax with the desired percentage. The cylinders thus obtained are submersed in water at room temperature (18-22° C.) and the effect obtained on the integrity of the cylinder is determined at different times. More information can be found on Example 14].

後処理

  1. customuntil melting in a reactor
  2. customprovided with a heating jacket and with mechanical stifling
  3. additionwas poured on a cylindrical mold
  4. waitleft
  5. temperatureto cool, in order

出典と根拠

ORDレコード
ord-1a1da7179e2b4f4a9ac7f6b9129a1f23
出典データセット
uspto-grants-2013_11
特許番号
US08585841B2

関連ノート

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