4-Nitrobenzaldehyde → HCID 178498134、化合物
反応式
[NH2:1][C:2]1[CH:11]=[CH:10][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:4][CH:3]=1.[N+:12]([C:15]1[CH:22]=[CH:21][C:18]([CH:19]=O)=[CH:17][CH:16]=1)([O-:14])=[O:13]>C(O)C>[N+:12]([C:15]1[CH:22]=[CH:21][C:18](/[CH:19]=[N:1]/[C:2]2[CH:3]=[CH:4][C:5]([C:6]([O:8][CH3:9])=[O:7])=[CH:10][CH:11]=2)=[CH:17][CH:16]=1)([O-:14])=[O:13]参加物
4
実験手順
A mixture of methyl 4-aminobenzoate (1.51 g, 10 mmol) and 4-nitrobenzaldehyde (1.51 g, 10 mmol) in ethanol (30 mL) was stirred overnight to give the yellow slurry. The precipitated off-white solid was collected and dried in vacuo to give (E)-methyl 4-(4-nitrobenzylideneamino)benzoate (2.93 g, 95% yield).
後処理
- customto give the yellow slurry
- customThe precipitated off-white solid was collected
- customdried in vacuo
出典と根拠
- ORDレコード
- ord-c1deb03f1a134b3bbbe26b09e2c5a64d
- 出典データセット
- uspto-grants-2013_11
- 特許番号
- US08586747B2
反応ノート
読み込み中…