化工社化工社 化学情報印刷レポート · 研究参考用
Potassium Permanganate → 3-Bromo-4-propoxybenzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Permanganate | HCID 516875 | — |
| 反応物 | 3-Bromo-4-propoxybenzaldehyde | HCID 4770041 | — |
| 生成物 | 3-Bromo-4-propoxybenzoic acid | HCID 8707153 | — |
反応手順
3-Bromo-4-propoxybenzaldehyde was oxidized by KMnO4, according to the procedure as described in Example 47, Step A, to give the title compound in 96%, as white solid. 1H-NMR (DMSO-d6) 0.98 (t, 3H, J=7.32 Hz); 1.68-1.79 (m, 2H); 4.06 (t, 2H, J=6.39 Hz); 7.14 (d, 1H, J=8.7 Hz); 7.87 (dd, 1H, J=2.07, 8.61 Hz); 8.01 (d, 1H, J=2.04 Hz); 11.2 (broad s, 1H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08592399B2 |
| 出典データセット | uspto-grants-2013_11 |
| ORD ID | ord-cb305201eb634e4fb5db335d915313c6 |
| 出典メモ | uspto-grants-2013_11 |