Ethanol → HCID 20344096、化合物

HRID 2049628ノート

反応式

HRID 2049628 の反応式
[F:1][C:2]1[CH:3]=[C:4]([CH:15]=[CH:16][CH:17]=1)[O:5][C:6]1[CH:14]=[CH:13][CH:12]=[CH:11][C:7]=1[C:8]([OH:10])=[O:9].OS(O)(=O)=O.[CH2:23](O)[CH3:24]>>[F:1][C:2]1[CH:3]=[C:4]([CH:15]=[CH:16][CH:17]=1)[O:5][C:6]1[CH:14]=[CH:13][CH:12]=[CH:11][C:7]=1[C:8]([O:10][CH2:23][CH3:24])=[O:9]

参加物

4

反応物 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 203440992-(3-Fluorophenoxy)benzoic acid

生成物 1

HCID 20344096HCID 20344096、化合物

実験手順

2-(3-Fluorophenoxy)benzoic acid (10 g.) and 100 ml of ethanol containing 1 ml. of concentrated H2SO4 were heated at reflux through molecular sieves overnight. The solvent was evaporated, and the residue poured into 50 ml. of 7% NaHCO3. The resulting ester was extracted with ether. ##STR10##

後処理

  1. temperatureat reflux through molecular sieves overnight
  2. customThe solvent was evaporated
  3. additionthe residue poured into 50 ml
  4. extractionThe resulting ester was extracted with ether

出典と根拠

ORDレコード
ord-34832fdf8e0e476fa5110ec0262fc185
出典データセット
uspto-grants-1980_04
特許番号
US04198421

反応ノート

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