Phenethylamine → 3-Methylthiopropan N-2-phenylethylamide
反応式
C[CH2:2][CH2:3][C:4](Cl)=[S:5].[C:7]1([CH2:13][CH2:14][NH2:15])[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>>[CH3:7][S:5][CH2:4][CH2:3][CH3:2].[C:7]1([CH2:13][CH2:14][NH-:15])[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1参加物
3
実験手順
Prepared from 3-methylthiopropionyl chloride (2.76 g) and 2-phenylethylamine (5.04 g) by the method used in Example 10(a). The solid product (3.79 g) was pure by t.l.c. A sample crystallised from aqueous methanol as needles m.p. 56°-59°.
後処理
- customA sample crystallised from aqueous methanol as needles m.p. 56°-59°
出典と根拠
- ORDレコード
- ord-2c699f3b86d548d88cacea4cb7971600
- 出典データセット
- uspto-grants-1980_04
- 特許番号
- US04199568
反応ノート
読み込み中…