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Propargylamine → HCID 178457545、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Propargylamine | HCID 239041 | — |
| 反応物 | Methyl 2-cyano-3,3-bis(methylsulfanyl)prop-2-enoate | HCID 319957 | — |
| 反応物 | HCID 178433288 | HCID 178433288 | — |
| 反応物 | HCID 178500817 | HCID 178500817 | — |
| 生成物 | HCID 178457545 | HCID 178457545 | — |
反応手順
When 1,1-bis(methylthio)-2-carbomethoxy-2-cyanoethylene [prepared according to the procedure described in Chem. Ber., 95, 2861 (1962)] is reacted with 2-[(4-methyl-1H-imidazol-5-yl)methylthio]ethylamine according to the procedure of Example 6, Step A, and the resultant 1-carbomethoxy-1-cyano-2-methylthio-2-{2-[(4-methyl-1H-imidazol-5-yl)methylthio]ethylamino}ethylene treated with propargylamine by the procedure of Example 6, Step B, there is produced 1-carbomethoxy-1-cyano-2-(2-propynylamino)-2-{2-[(4-methyl-1H-imidazol-5-yl)methylthio]ethylamino}ethylene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04200760 |
| 出典データセット | uspto-grants-1980_04 |
| ORD ID | ord-a0882c7dd16b4ad3abd3ddf46574ad93 |
| 出典メモ | uspto-grants-1980_04 |