化工社化工社 化学情報印刷レポート · 研究参考用
Hydrogen Peroxide → N,N-ditetradecylhydroxylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Peroxide | HCID 784 | — |
| 反応物 | Dimyristylamine | HCID 87077 | — |
| 溶媒 | 1-Propanol | HCID 1031 | — |
| 生成物 | N,N-ditetradecylhydroxylamine | HCID 9910313 | — |
反応手順
The general procedure of Example 5 is followed using, at 50 to 55° C., 50 grams (0.12 mol) of ditetradecylamine, 200 ml of n-propanol and 8.3 grams (0.12 mol) of 50% aqueous hydrogen peroxide solution. The above-named product is obtained in a yield of 33.4 grams (64%) as white needles melting at 97-99° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05013510 |
| 出典データセット | uspto-grants-1991_05 |
| ORD ID | ord-8eab5f4823ab4de0adb46b17be783994 |
| 出典メモ | uspto-grants-1991_05 |