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2,6-Difluorobenzoyl chloride → ethyl N-(2,6-difluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Difluorobenzoyl chloride | HCID 87438 | — |
| 反応物 | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate | HCID 19833914 | — |
| 生成物 | ethyl N-(2,6-difluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 19834014 | — |
反応手順
starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and 2,6-difluorobenzoyl chloride, there is obtained ethyl N-(2,6-difluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a resin, mass spectrum m/e: M+ 406 (5), 377 (21), 194 (100), 141 (42);
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05015640 |
| 出典データセット | uspto-grants-1991_05 |
| ORD ID | ord-2cb39286482e4f9794a27f841e2c1abe |
| 出典メモ | uspto-grants-1991_05 |