4-Fluorobenzoyl chloride → isopropyl N-(p-fluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
反応式
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:21])[O:17][CH:18]([CH3:20])[CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[F:22][C:23]1[CH:31]=[CH:30][C:26]([C:27](Cl)=[O:28])=[CH:25][CH:24]=1>>[F:22][C:23]1[CH:31]=[CH:30][C:26]([C:27]([N:21]=[C:16]([N:7]2[CH2:6][C:5]3[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=3[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8]2)[O:17][CH:18]([CH3:19])[CH3:20])=[O:28])=[CH:25][CH:24]=1参加物
3
実験手順
starting from isopropyl 5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate and p-fluorobenzoyl chloride, there is obtained isopropyl N-(p-fluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate, m.p. 90°-93° C.;
出典と根拠
- ORDレコード
- ord-d0c23c155deb4a19b651bd88998b5efc
- 出典データセット
- uspto-grants-1991_05
- 特許番号
- US05015640
反応ノート
読み込み中…