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p-(Trifluoromethoxy)phenyl isocyanate → ethyl N-{[p-(trifluoromethoxy)-phenyl]carbamoyl}-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-(Trifluoromethoxy)phenyl isocyanate | HCID 92298 | — |
| 反応物 | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate | HCID 19833914 | — |
| 生成物 | ethyl N-{[p-(trifluoromethoxy)-phenyl]carbamoyl}-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 67929433 | — |
反応手順
starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and p-(trifluoromethoxy)-phenyl isocyanate, there is obtained ethyl N-{[p-(trifluoromethoxy)-phenyl]carbamoyl}-5,7-dihydro-6H-dibenz[c,e]azepine-6 -carboximidate, m.p. 129°-130° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05015640 |
| 出典データセット | uspto-grants-1991_05 |
| ORD ID | ord-c3a0d783706c40a8aa7b3990f3de05c1 |
| 出典メモ | uspto-grants-1991_05 |