Methyl behenate → Potassium Behenate

HRID 2051147

反応式

HRID 2051147 の反応式
[C:1]([O:24]C)(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[OH-].[K+:27]>CO>[C:1]([O-:24])(=[O:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[K+:27]

参加物

4

反応物 2

HCID 13584Methyl behenateHCID 14797Potassium Hydroxide

生成物 1

HCID 23663647Potassium Behenate

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

Methyl behenate (0.375 moles/mole of sucrose to be used in Step B) is saponified by stirring at reflux in methanol containing an equivalent amount of KOH. The reaction is stirred with heating until all methyl ester has been converted to soap as indicated by infrared analysis. The soap solution is used, as is in the next reaction step.

後処理

  1. stirringThe reaction is stirred
  2. customas is in the next reaction step

出典と根拠

ORDレコード
ord-0d593acef01e4db580c4d465cab66206
出典データセット
uspto-grants-1991_05
特許番号
US05017398

関連ノート

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