Hydrochloric Acid → HCID 23452782、化合物
反応式
[CH2:1]([C:5]1(O)[C:10]([CH3:12])(C)[CH2:9][C:8](=[O:13])[CH:7]=[C:6]1[CH3:14])[CH2:2][CH2:3][CH3:4].Cl.[C:17]1(=O)C=CCC=C1>CCCCCC>[CH2:1]([C:5]1([CH3:17])[C:6]([CH3:14])=[CH:7][C:8](=[O:13])[CH:9]=[C:10]1[CH3:12])[CH2:2][CH2:3][CH3:4]参加物
5
実験手順
A solution of 7 g of 4-butyl-4-hydroxy-3,5,5-trimethyl-2-cyclohexen-1-one (prepared by the procedure of Example IV) in hexane is stirred overnight with 10 ml of a 5% solution of HCl. The hexane is separated and evaporated, and the residue is distilled through a micro column using triethanolamine as a still base. The product obtained is 4-butyl-3,4,5-trimethyl-(2,5-cyclohexadien-1-one, boiling point 112°-119° C. at 0.1 mm Hg. The compound exhibits the following spectral characteristics:
後処理
- customThe hexane is separated
- customevaporated
- distillationthe residue is distilled through a micro column
- customThe product obtained
出典と根拠
- ORDレコード
- ord-3803d517a6ae41ca900784ad02d69493
- 出典データセット
- uspto-grants-1980_01
- 特許番号
- US04186149
反応ノート
読み込み中…