Hydrochloric Acid → HCID 12282158、化合物
反応式
[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[CH:4][CH:3]=1.[CH2:10]([O:12]CC)[CH3:11].Cl>C(O)C>[ClH:1].[CH2:10]([O:12][C:6](=[NH:7])[C:5]1[CH:8]=[CH:9][C:2]([Cl:1])=[CH:3][CH:4]=1)[CH3:11]参加物
5
実験手順
10 g of 4-chlorobenzonitrile was suspended in 12 ml of ethanol and dissolved by adding diethyl ether. While being cooled in an ice bath, it was saturated with HCl gas. After 72 hours, precipitated product was suctioned out. The product was washed with diethyl ether.
後処理
- dissolutiondissolved
- temperatureWhile being cooled in an ice bath
- customprecipitated product
- washThe product was washed with diethyl ether
出典と根拠
- ORDレコード
- ord-231563f31ae040c99aa98ef43e98b912
- 出典データセット
- uspto-grants-2008_02
- 特許番号
- US07329679B2
反応ノート
読み込み中…