(S)-1-(4-Methoxyphenyl)ethylamine → HCID 12083219、化合物

反応式

[C:1]1([S:7]([NH:10][C:11]2[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][C:12]=2[C:13](Cl)=[O:14])(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:21][C@H:22]([NH2:31])[C:23]1[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=1>>[C:1]1([S:7]([NH:10][C:11]2[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][C:12]=2[C:13]([NH:31][C@H:22]([C:23]2[CH:28]=[CH:27][C:26]([O:29][CH3:30])=[CH:25][CH:24]=2)[CH3:21])=[O:14])(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

参加物

反応物 2

HCID 793467(S)-1-(4-Methoxyphenyl)ethylamine

HCID 120832222-Phenylsulfonylamino-5-chlorobenzoyl chloride

生成物 1

HCID 12083219HCID 12083219、化合物

実験手順

136 mg of the title compound were obtained from 2-phenylsulfonylamino-5-chlorobenzoyl chloride and S-(−)-1-(4-methoxyphenyl)ethylamine in accordance with general method 5. MS (ES+): m/z=445 (M+1).

出典と根拠

ORDレコード: ord-706e07bfeccc44b0afd91004220a1e42
出典データセット: uspto-grants-2008_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07332608B2

反応ノート

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