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(3R)-3-methyl-1-(1H,3H-naphtho[1,8-cd]pyran-6-yl)piperazine → (3R)-3-methyl-1-(1H,3H-naphtho[1,8-cd]thiopyran-6-yl)piperazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (3R)-3-methyl-1-(1H,3H-naphtho[1,8-cd]pyran-6-yl)piperazine | HCID 69306502 | — |
| 反応物 | 6-bromo-1H,3H-naphtho[1,8-cd]thiopyran | HCID 69307792 | — |
| 生成物 | (3R)-3-methyl-1-(1H,3H-naphtho[1,8-cd]thiopyran-6-yl)piperazine | HCID 69307284 | — |
反応手順
The procedure used for the synthesis of (3R)-3-methyl-1-(1H,3H-naphtho[1,8-cd]pyran-6-yl)piperazine (Example 5b)) was followed, using 6-bromo-1H,3H-naphtho[1,8-cd]thiopyran as starting material and making non-critical variations, to obtain the title compound (3R)-3-methyl-1-(1H,3H-naphtho[1,8-cd]thiopyran-6-yl)piperazine as brown solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07335660B2 |
| 出典データセット | uspto-grants-2008_02 |
| ORD ID | ord-2a669c62074d4c03baaea38a701ea01b |
| 出典メモ | uspto-grants-2008_02 |