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Sodium Carbonate → 4-Hydroxyisophthalic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | 4-Bromo-1,3-benzenedicarboxylic acid | HCID 81361 | — |
| 生成物 | 4-Hydroxyisophthalic acid | HCID 12490 | 82% |
反応手順
The same procedure as described in Example 24 was performed but using 2.45 g (10.0 mmol) of 4-bromoisophthalic acid as the substrate and 2.70 g (25.5 mmol) of Na2CO3 instead of Ca(OH)2. A total of 1.49 g (8.2 mmol, 82% yield) of 4-hydroxyisophthalic acid was collected. The purity was determined by 1H NMR to be 88%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07335791B1 |
| 出典データセット | uspto-grants-2008_02 |
| ORD ID | ord-44522d51b97047ea93e84d115d3643eb |
| 出典メモ | uspto-grants-2008_02 |